Search results for " Titanium"

showing 10 items of 126 documents

Formation of dibutyl carbonate and butylcarbamate via CO2 insertion in titanium(IV) butoxide and reaction with n-butylamine

2016

Abstract The species resulting from insertion of 12CO2 and 13CO2 into titanium(IV) butoxide is for the first time fully characterized by means of infrared and nuclear magnetic resonance spectroscopy. Results show formation of Ti-monobutylcarbonate, that easily undergoes nucleophilic attack by an aliphatic amine. The hydrolysis of the resulting species produces butylcarbamate and dibutylcarbonate as the only main products. Characterization results of the carbonate-like adduct, along with its reactivity with amine molecules open the route to new ways of CO2 utilization as building block for valuable organic compounds.

010405 organic chemistryChemistryProcess Chemistry and Technologyn-Butylaminechemistry.chemical_elementNuclear magnetic resonance spectroscopy010402 general chemistry01 natural sciences0104 chemical sciencesAdductHydrolysischemistry.chemical_compoundNucleophilePolymer chemistryChemical Engineering (miscellaneous)Organic chemistryReactivity (chemistry)Amine gas treatingSettore CHIM/07 - Fondamenti Chimici Delle TecnologieWaste Management and DisposalTitaniumDibutyl carbonate CO2 insertion Titanium alkoxides Carbamate
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Effect of TiO2 nanoparticles in thyme under reduced irrigation conditions

2018

The nanotechnology is a relatively new technology that has recently entered the field of agriculture. Nanotechnology covers the integration or manipulation of individual atoms, molecules or molecular masses to a diverse array of structures allowing the production of new characteristics and traits of interest. The aim of this study was to evaluate the effects of foliar application of TiO2 nanoparticles on quantitative traits (plant height, number of branches, dry weight of shoots and roots) and the essential oil content of thyme under different levels of field capacity. Our results showed that the application of TiO2 nanoparticles had significant effects on thyme growth, while the essential …

0106 biological sciences0301 basic medicineIrrigationThymus vulgarislcsh:TX341-64101 natural sciencesessencelaw.inventionField capacity03 medical and health sciencesThymus vulgarisDry weightlawEssential oilbiologybusiness.industryTio2 nanoparticlesbiology.organism_classificationHorticulture030104 developmental biologyAgricultureShootnano dioxide titaniumbusinesslcsh:Nutrition. Foods and food supplyreduced irrigation010606 plant biology & botanyFood SciencePotravinarstvo Slovak Journal of Food Sciences
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Single block 3D numerical model for linear friction welding of titanium alloy

2018

A two-stage approach for the simulation of Linear Friction Welding is presented. The proposed model, developed using the commercial simulation package DEFORM, is 3D Lagrangian, thermo-mechanically coupled. The first phase of the process was modelled with two distinct workpieces, while the remaining phases were simulated using a single-block model. The Piwnik–Plata criterion was set up and used to determine the shifting from the dual object to the single-block model. The model, validated against experimental temperature measurements, is able to predict the main field variables distributions with varying process parameters. Titanium alpha and beta phases evolution during the whole process has…

0209 industrial biotechnologyMaterials scienceFinite element method titanium linear friction welding Ti6Al4VTitanium alloychemistry.chemical_element02 engineering and technology021001 nanoscience & nanotechnologyCondensed Matter PhysicsFinite element methodsymbols.namesake020901 industrial engineering & automationchemistryBlock (telecommunications)symbolsGeneral Materials ScienceFriction weldingComposite material0210 nano-technologySettore ING-IND/16 - Tecnologie E Sistemi Di LavorazioneLagrangianTitanium
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An in vitro cyclic fatigue resistance comparison of conventional and new generation nickel-titanium rotary files

2018

Background New designs and processing of Niquel-Titanium (NiTi) have been introduced to increase resistance to cyclic fatigue. The purpose of this study was to compare the cyclic fatigue resistance of 3 NiTi rotary instruments, ProTaper Next (PTN; Dentsply Maillefer, Ballaigues, Switzerland), Profile Vortex Blue (PVB; Dentsply Tulsa Dental, Tulsa, OK, USA) and ProTaper Universal (PTU; Dentsply Maillefer, Ballaigues, Switzerland). Material and Methods A cyclic fatigue test was conducted operating instruments from ProTaper Next X2, Profile Vortex Blue 25.06 and ProTaper F2. A total of 234 instruments were rotated in 2 simulated stainless steel curved canals with different angles of curvature …

0301 basic medicine03 medical and health sciencesCyclic stress030104 developmental biology0302 clinical medicineMaterials scienceNickel titaniumManufacturing processUNESCO::CIENCIAS MÉDICAS030206 dentistryComposite material:CIENCIAS MÉDICAS [UNESCO]General DentistryJournal of Clinical and Experimental Dentistry
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Implant Abutment Cleaning by Plasma of Argon: 5-Year Follow-Up of a Randomized Controlled Trial.

2015

Contamination of implant abutments could potentially influence the peri-implant tissue inflammatory response. The aim of the present study is to assess the radiographic bone changes around customized, platform-switched abutments placed according to the "one-abutment-one-time" protocol, with and without plasma of argon cleaning treatment.Thirty healthy patients with thin gingival biotype (1 mm) and history of periodontal disease received one maxillary implant each. Immediately before abutment connection, patients were randomly assigned to control group (cleaning protocol by steaming) or test group (plasma of argon treatment). Outcome measures were: 1) success rate of implants and prostheses;…

0301 basic medicine5 year follow upRadiographyAbutmentAlveolar Bone LossDentistryDental AbutmentsOsseointegrationlaw.invention03 medical and health sciences0302 clinical medicineDental Implants Single-ToothDental AbutmentsRandomized controlled triallawestheticsMedicineHumanstitaniumArgondental implant platform switchingbusiness.industry030206 dentistryArgon; bone resorption; dental implant-abutment interface; dental implant platform switching; esthetics; titanium.dental implant-abutment interface030104 developmental biologyPeriodonticsImplantbusinessbone resorptionImplant abutmentFollow-Up StudiesJournal of periodontology
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Quantitative and Qualitative in vivo Analysis of Metal Residuals in the Saliva of Subjects with and without Fixed Orthodontic Appliances

2020

Aim of the Work: The aim of this work was to evaluate Ni e Cr ions in the saliva of subjects with and without fixed orthodontic appliances. Materials and Methods: This was a prospective, non-randomized study of 100 patients, so selected: 50 have undergone fixed orthodontic appliance at least from 24 months; others 50 subjects as control-group, without any fixed and/or removable orthodontic appliance It was conducted according to the Declaration of the World Medical Association of Helsinki. The two selected groups were compatible for age, sex, absence of restoration in amalgam or other metals in the oral cavity. The saliva of all the subjects was collected with standardized sterile methods. …

0301 basic medicineSalivaMaterials scienceMetal ions in aqueous solutionfungiMetallurgytechnology industry and agriculture030206 dentistryGeneral MedicineBiocompatible materialCorrosionMetal03 medical and health sciences030104 developmental biology0302 clinical medicineNickel titaniumFixed Orthodontic Appliancevisual_artGalvanic cellvisual_art.visual_art_mediumNickel ionsAtomic Absorption SpectrophotometryMetal IonSaliva
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Corrosion and wear resistance of coatings produced on AZ31 Mg alloy by plasma electrolytic oxidation in silicate-based K2TiF6 containing solution: Ef…

2022

Abstract In this research, plasma electrolytic oxidation coatings were prepared on AZ31 Mg alloy in a silicate-based solution containing K2TiF6 using bipolar and soft sparking waveforms with 10, 20, and 30% cathodic duty cycles. The coatings displayed a net-like surface morphology consisted of irregular micro-pores, micro-cracks, fused oxide particles, and a sintered structure. Due to the incorporation of TiO2 colloidal particles and the cathodic pulse repair effect, most of the micro-pores were sealed. Long-term corrosion performance of the coatings was investigated using electrochemical impedance spectroscopy during immersion in 3.5 wt.% NaCl solution up to 14 days. The coating grown by t…

AZ31 Mg alloyWear resistanceMaterials scienceAlloyPlasma electrolytic oxidationMetals and AlloysOxideCorrosion resistancePulsed waveformPlasma electrolytic oxidationengineering.materialCathodic protectionCorrosionDielectric spectroscopychemistry.chemical_compoundSettore ING-IND/23 - Chimica Fisica ApplicatachemistryCoatingMechanics of MaterialsengineeringComposite materialLayer (electronics)Dipotassium titanium hexafluoride
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Skull Bone Defects Reconstruction with Custom-Made Titanium Graft shaped with Electron Beam Melting Technology: Preliminary Experience in a Series of…

2017

Background: Cranioplasty represents a challenge in neurosurgery. Its goal is not only plastic reconstruction of the skull but also to restore and preserve cranial function, to improve cerebral hemodynamics, and to provide mechanical protection of the neural structures. The ideal material for the reconstructive procedures and the surgical timing are still controversial. Many alloplastic materials are available for performing cranioplasty and among these, titanium still represents a widely proven and accepted choice. Methods: The aim of our study was to present our preliminary experience with a “custom-made” cranioplasty, using electron beam melting (EBM) technology, in a series of ten patien…

AdultMaleDecompressive Craniectomymedicine.medical_treatmentchemistry.chemical_elementDentistryNeurosurgical ProceduresCranioplasty030218 nuclear medicine & medical imagingProsthesis Implantation03 medical and health sciencesImaging Three-Dimensional0302 clinical medicineFreezingElectron beam melting technologymedicineHumansSkull boneReconstructive Surgical ProceduresCustom-made titanium implantsAgedRetrospective StudiesTitaniumSettore MED/27 - Neurochirurgiabusiness.industrySkullMiddle AgedCranioplastySkullmedicine.anatomical_structurechemistry3D computer-aided design and computer-aided manufacturing (CAD/CAM) technologiesCerebral hemodynamicsComputer-Aided DesignFemaleSkull bone defectsTomography X-Ray Computedbusiness030217 neurology & neurosurgeryTitaniumBiomedical engineering
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TITAFORM - Precision Hot Forming, development of innovative hot-forming processes of aeronautical components in Ti-alloy with low buy/fly ratio: an I…

2012

In the paper the description of the project TITAFORM is provided. The project has been financed on the call "PON Linea 1" of the Italian government and represents an effective example of cooperation between academy and industry. The project is focused on the beta forging and hot stretch forming operations of titanium alloys. �� 2012 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Aeronautical components Beta forging Hot forming Magnesium alloy sheets Stretch-forming Ti alloyForging Titianium Phases transformationMetal formingMagnesium alloys Titanium alloys Upsetting (forming)Settore ING-IND/16 - Tecnologie E Sistemi Di Lavorazione
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Visible Light Induced Sulfoxidation of Alkanes in the Presence of Titania

2012

Alkanes titanium dioxide C-H activation photocatalysis sulfoxidation sulfur dioxide
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